Title | Determination of Cu and Pb concentrations based on urease activity inhibition of Durio zibethinus L. seeds |
Author Order | 3 of 4 |
Accreditation | |
Abstract | The determination of heavy metal concentrations has been carried out using sophisticated instruments, and therefore a simple and reliable alternative method is needed as a comparison. The study aimed to determine Cu and Pb concentration of standard solution using the urease activity inhibition method ofÃÂÃÂ Durio zibethinusÃÂÃÂ L.ÃÂÃÂ ÃÂÃÂ seeds.ÃÂÃÂ ÃÂÃÂ The research started with urease extraction fromÃÂÃÂ DurioÃÂÃÂ D.ÃÂÃÂ zibethinusÃÂÃÂ L.ÃÂÃÂ seeds. The activity of the obtained extract was determined using the Nessler method. The optimum substrate concentration was also determined. Urease activity inhibition was carried out using various metal solution concentrations, which continued by plotting a log graph of urea concentration vs. %inhibition. The obtained graph would then determine the metal concentration in a synthetic water sample.ÃÂÃÂ The data was then compared to the measurement, determined by the Atomic Absorption Spectrophotometry (AAS) method.ÃÂÃÂ Results of the study showed that the urease activity ofÃÂÃÂ D. zibethinusÃÂÃÂ L.seeds was 296.774 U/mL. Urease activity was optimum at a urea concentration of 0.3 M. The comparisonÃÂÃÂ Cu, and PbÃÂÃÂ concentration determination using the urease inhibitory activity and AAS methods showed no significant difference at 95% confidence level. This research showed that urease ofÃÂÃÂ D. zibethinusÃÂÃÂ L. seed could be used to determine Cu and Pb's concentration based on its inhibiting activity. |
Publisher Name | Universitas Jenderal Soedirman |
Publish Date | 2021-07-20 |
Publish Year | 2021 |
Doi | DOI: 10.20884/1.jm.2021.16.2.736 |
Citation | |
Source | Molekul |
Source Issue | Vol 16, No 2 (2021) |
Source Page | 92-99 |
Url | https://ojs.jmolekul.com/ojs/index.php/jm/article/view/736/376 |
Author | DIAN RIANA NINGSIH, S.Si, M.Si |
File | 2097824.pdf |
---|